Janickis V1, Necas M, Novosad J, Dusek M, Petrícek V.
Acta Crystallogr B. 2002 Dec;58(Pt 6):977-85. Epub 2002 Nov 28.Structure analysis of [(C(2)H(5))(n)(C(6)H(5))(4-n)P](2)[TeBr(6)(Se(2)Br(2))(2)] is presented for n = 1 and 0 [hereafter (I) and (II)]. Crystal (I) has been synthesized from elemental selenium, tellurium tetrabromide, ethyltriphenylphosphonium bromide and bromine. It has a standard monoclinic structure, space group P2(1)/c, and has been solved and refined to R = 0.0357 for 4803 observed X-ray reflections by traditional techniques. Read More