Corrigan DK1, Blair EO, Terry JG, Walton AJ, Mount AR.
Anal Chem. 2014 Nov 18;86(22):11342-8. doi: 10.1021/ac5030842. Epub 2014 Oct 24.Molten salts (MSs) are an attractive medium for chemical and electrochemical processing and as a result there is demand for MS-compatible analysis technologies. However, MSs containing redox species present a challenging environment in which to perform analytical measurements because of their corrosive nature, significant thermal convection and the high temperatures involved. This paper outlines the fabrication and characterization of microfabricated square microelectrodes (MSMs) designed for electrochemical analysis in MS systems. Read More