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Lithium ammonia borane | CAS Number: 99144-67-9

Catalog Number
ACM99144679
Product Name
Lithium ammonia borane
Structure
CAS Number
99144-67-9
IUPAC Name
lithium;azanide;boron
Synonyms
Lithium ammonia borane;Lithium ammonia borane technical grade
Molecular Weight
37.80634
Exact Mass
37.06750
Molecular Formula
BH6LiN
Purity
96%
SMILES
[Li+].[B].[NH2-]
InChIKey
ZLLCRZMXMAVHSG-UHFFFAOYSA-N
H-Bond Donor
1
H-Bond Acceptor
1
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1One-pot synthesis of ammonia-borane and trialkylamine-boranes from trimethyl borate.

Ramachandran PV1, Raju BC, Gagare PD.

Org Lett. 2012 Dec 21;14(24):6119-21. doi: 10.1021/ol302421t. Epub 2012 Dec 5.

A one-pot procedure for the preparation of ammonia borane from trimethyl borate in 90% yield and >99% purity has been reported. This methodology has been modified to prepare a series of trialkylamine-boranes in 70-82% yields from trimethyl borate and lithium hydride/aluminum chloride in the presence of the corresponding trialkylamine.

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Email:
Tel:1-201-478-8534
1-516-662-5404
Fax: 1-516-927-0118
Address: Suite 212, Waverly Plaza, 755 Waverly Avenue, Holtsville, NY 11742, USA