Boczkaj G1, Makoś P2, Fernandes A2, Przyjazny A3.
J Sep Sci. 2016 Oct;39(20):3946-3956. doi: 10.1002/jssc.201600608. Epub 2016 Sep 22.We present a new procedure for the determination of volatile organosulfur compounds in samples of industrial effluents using dispersive liquid-liquid microextraction and gas chromatography with flame photometric detection. Initially, the extraction parameters were optimized. These included: type and volume of extraction solvent, volume of disperser solvent, salting out effect, pH, time and speed of centrifugation as well as extraction time. Read More